(12) Translation of european patent specification

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1 (12) Translation of european patent specification (11) NO/EP B1 (19) NO NORWAY (1) Int Cl. B01D 3/00 ( ) B01D 3/74 ( ) C02F 1/66 ( ) Norwegian Industrial Property Office (21) Translation Published (80) Date of The European Patent Office Publication of the Granted Patent (86) European Application Nr (86) European Filing Date (87) The European Application s Publication Date (30) Priority , EP, , EP, (84) Designated Contracting States: AL AT BE BG CH CY CZ DE DK EE ES FI FR GB GR HR HU IE IS IT LI LT LU LV MC MK MT NL NO PL PT RO RS SE SI SK SM TR (73) Proprietor PureteQ A/S, Norgesvej 13 Tved, 700 Svendborg, DK-Danmark Søgaard, Dennis, Majas Vej 21 Humlum, 7600 Struer, DK-Danmark (72) Inventor SØGAARD, Dennis, Majas Vej 21Humlum, DK-7600 Struer, DK-Danmark (4) Title METHOD FOR REMOVING IMPURITIES FROM FLUE GAS CONDENSATE (6) References Cited: WO-A1-81/00277 DE-A DE-A DE-A DE-A US-A

2 Enclosed is a translation of the patent claims in Norwegian. Please note that as per the Norwegian Patents Acts, section 66i the patent will receive protection in Norway only as far as there is agreement between the translation and the language of the application/patent granted at the EPO. In matters concerning the validity of the patent, language of the application/patent granted at the EPO will be used as the basis for the decision. The patent documents published by the EPO are available through Espacenet ( or via the search engine on our website here: NO/EP

3 1 PATENTKRAV 1. Framgangsmåte for å behandle røykgass eller røykgasskondensater, som innbefatter: et første trinn der det tilveiebringes en røykgass og/eller et røykgasskondensat som innbefatter svovelholdige forbindelser, et andre trinn der røykgassen og/eller røykgasskondensatet bringes i kontakt med et kalsiumholdig materiale, et tredje trinn der væsken som dannes i trinn to gjennomgår et kjøletrinn slik at den kjøles til 60 C eller lavere, 1 et fjerde trinn der ph justeres til 6 9 ved å tilsette et andre materiale og dermed la det felles et første kalsium- og svovelholdig bunnfall og dannes en første flytende supernatant, 20 et femte trinn der det første bunnfallet skilles fra den første supernatanten fra det fjerde trinnet ved gravitasjonssedimentering eller sentrifugering. 2. Framgangsmåte ifølge krav 1, der ph i det andre trinnet justeres ved å tilsette et basisk kalsiumholdig materiale slik at ph blir liggende i et område mellom 11 og 14, og dermed tilveiebringe et basisk røykgasskondensat Framgangsmåte ifølge ett av trinnene 1 og 2, der røykgassen fås ved forbrenning av biologisk brensel, for eksempel flis, høy eller ved, ved søppelforbrenning, som eksos fra forbrenningsmotorer, ved gassforbrenning, oljeproduksjon eller fra energibriketter. 4. Framgangsmåte ifølge ett av de foregående kravene, der røykgassen eller røykgasskondensatet som tilveiebringes i trinn 1, inneholder én eller flere forurensninger valgt fra gruppen som innbefatter flygeaske, svovelsalter og tungmetaller som bly-, kadmium-, kvikksølv- og bariumsalter.

4 2. Framgangsmåte ifølge noen av de foregående kravene, der røykgassen eller kondensatet tilveiebringes ved å senke temperaturen i røykgassen til under 90 C ved varmeveksling mellom røykgassen og en væske som skal varmes opp ved den brenningen av brensel som danner røykgassen. 6. Framgangsmåte ifølge noen av de foregående kravene, der det kalsiumholdige materialet eller det kalsiumholdige basiske materialet er en vannsuspensjon eller vannløsning av Ca(OH) 2, CaO eller CaCO 3 eller en blanding av disse. 7. Framgangsmåte ifølge noen av de foregående kravene, der det andre materialet er en gass som innbefatter CO 2, og denne gassen bobles gjennom det basiske røykgasskondensatet som tilveiebringes i trinn Framgangsmåte ifølge krav 7, der CO 2 -kontaktgassen inneholder minst 00 volum-ppm CO Framgangsmåte ifølge noen av de foregående kravene, der det andre trinnet der det tilsettes et kalsiumholdig basisk materiale slik at ph i røykgasskondensatet som tilveiebringes i trinn 1, justeres til ph for å tilveiebringe en basisk røykgass eller et basisk røykgasskondensat, utføres ved å tilsette røykgassen eller røykgasskondensatet som tilveiebringes i trinn 1 til et kalsiumholdig basisk materiale med konstant justert ph på Framgangsmåte ifølge noen av kravene 1 9, der røykgassen eller røykgasskondensatet bringes i kontakt med et kalsiumholdig materiale som er en vandig vaskevæske, i en vaskesone, slik at svovelholdige gasser i væsken absorberes. 11. Framgangsmåte ifølge noen av kravene 1 9, der det etter det andre trinnet direkte etableres en minst partiell strøm av væske som stammer fra det andre trinnet, til en første gjenvinningssone, slik at vaskevæsken dermed gjenvinnes.

5 3 12. Framgangsmåte ifølge noen av kravene 1 9 og 11, som også innbefatter: et sjette trinn der en første partiell strøm av den første flytende supernatanten som stammer fra det første trinnet, resirkuleres til vaskesonen ifølge krav 11 for å absorbere mer svovelholdig gass, et sjuende trinn der det etableres en andre partiell strøm av den første flytende supernatanten som stammer fra det femte trinnet, til en andre gjenvinningssone, slik at vaskevæsken dermed kan gjenvinnes, 1 et åttende trinn der væsken i den andre gjenvinningssonen tilsettes CaO, CaCO 3, Ca(OH) 2 og/eller en blanding av disse, for å justere ph i væsken til 9 14, slik at det dannes et andre bunnfall som inneholder svovel og en andre flytende supernatant, et niende trinn der det andre bunnfallet skilles fra den andre flytende supernatanten, 20 et tiende trinn der den andre flytende supernatanten som stammer fra det niende trinnet, bringes i kontakt med en CO 2 -holdig gass, for å senke ph i væsken til et intervall fra rundt til rundt 8, 2 et ellevte trinn der den resulterende flytende supernatanten som stammer fra det tiende trinnet, slippes ut i et kloakksystem. 13. Framgangsmåte ifølge krav 12, der det brukes Ca(OH) 2 i det fjerde og i det åttende trinnet Framgangsmåte ifølge noen av kravene ovenfor, der det femte trinnet utføres ved å sedimentere bunnfallet i to eller flere sedimenteringstanker som har fluid forbindelse med hverandre.

6 4 1. Framgangsmåte ifølge noen av kravene ovenfor, der den CO 2 - holdige gassen i det tiende trinnet er forbrenningsgass fra en forbrenningsanordning, eventuelt blandet med omgivelsesluft. 16. Framgangsmåte ifølge noen av kravene 12 1 ovenfor, der den første partielle strømmen i det sjette trinnet er minst fem ganger så stor som den andre partielle strømmen i det sjuende trinnet, uttrykt i volum per tidsenhet. 17. Framgangsmåte ifølge noen av kravene 1 9 ovenfor, der det fjerde trinnet også innbefatter å boble væsken med en CO 2 -holdig gass etter at ph i væsken er justert til 6 8 ved å tilsette CaO, CaCO 3, Ca(OH) 2 og/eller en blanding av disse.

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