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1 (12) Translation of european patent specification (11) NO/EP B1 (19) NO NORWAY (1) Int Cl. C01B 33/037 ( ) Norwegian Industrial Property Office (21) Translation Published (80) Date of The European Patent Office Publication of the Granted Patent (86) European Application Nr (86) European Filing Date (87) The European Application s Publication Date (30) Priority , US, P (84) Designated Contracting States: AT BE BG CH CY CZ DE DK EE ES FI FR GB GR HR HU IE IS IT LI LT LU LV MC MT NL NO PL PT RO SE SI SK TR (73) Proprietor Silicio Ferrosolar, S.L.U., Paseo de la Castellana 29-D Planta 49 4 Torres Business Area, Torre Espacio, Madrid, ES-Spania (72) Inventor LEBLANC, Dominic, 239, Ave du Sagittaire, Bécancour, Québec G9H 4J4, CA- Canada BOISVERT, René, 230, boul. du Carmel, Trois-Rivières, Québec G8Z 3S2, CA- Canada (74) Agent or Attorney Bryn Aarflot AS, Postboks 449 Sentrum, 0104 OSLO, Norge (4) Title Fremgangsmåte for fremstilling av silisium med middels og høy renhet fra silisium av metallurgisk kvalitet (6) References Cited: GB-A JP-A US-A US-A

2 Enclosed is a translation of the patent claims in Norwegian. Please note that as per the Norwegian Patents Acts, section 66i the patent will receive protection in Norway only as far as there is agreement between the translation and the language of the application/patent granted at the EPO. In matters concerning the validity of the patent, language of the application/patent granted at the EPO will be used as the basis for the decision. The patent documents published by the EPO are available through Espacenet (http://worldwide.espacenet.com) or via the search engine on our website here: https://search.patentstyret.no/ NO/EP

3 1 P a t e n t k r a v Fremgangsmåte for å rense silisium av metallurgisk kvalitet med lav renhet, inneholdende minst én av følgende kontaminanter Al, As, Ba, Bi, Ca, Cd, Fe, Co, Cr, Cu, Fe, La, Mg, Mn, Mo, Na, Ni, P, Pb, Sb, Sc, Sn, Sr, Ti, V, Zn, Zr og B, og frembringe et fast polykrystallinsk silisium med høyere renhet, idet nevnte fremgangsmåte omfatter de trinn å: (a) inneholde en smelte av silisium av metallurgisk kvalitet med lav renhet i en form, idet nevnte form har en isolert bunnvegg, isolerte sidevegger og en åpen topp; (b) størkne smelten gjennom ensrettet størkning fra nevnte åpne topp mot nevnte isolerte bunnvegg i nevnte form mens smelten omrøres elektromagnetisk; (c) styre en hastighet av nevnte ensrettede størkning; (d) stanse nevnte ensrettede størkning når smelten har delvis størknet for å danne en støpeblokk som har et ytre skall omfattende nevnte faste polykrystallinske silisium med høyere renhet og et senter omfattende et urenhet-anriket flytende silisium; og (e) danne en åpning i nevnte ytre skall til nevnte støpeblokk for å slippe ut nevnte urenhet-anrikede flytende silisium og etterlate det ytre skallet omfattende nevnte faste polykrystallinske silisium med høyere renhet og med det frembringe nevnte faste polykrystallinske silisium med høyere renhet Fremgangsmåte ifølge krav 1, hvor nevnte isolerte bunnvegg og nevnte isolerte sidevegger varmes opp for å minimere dannelse av en overflate av silisium på nevnte isolerte bunnvegg og nevnte isolerte sidevegger i nevnte form. 3. Fremgangsmåte ifølge krav 1, hvor nevnte hastighet av ensrettet størkning styres gjennom en isolering av nevnte isolerte bunnvegg og nevnte isolerte sidevegger Fremgangsmåte ifølge krav 1, hvor nevnte hastighet av ensrettet størkning styres ved å styre en varmeuttrekkingshastighet fra smelten ved nevnte åpne topp av nevnte form. 3. Fremgangsmåte ifølge krav 4, hvor det å styre en varmeuttrekkingshastighet omfatter å anbringe et kjølemedium i kontakt med en fri overflate av smelten ved nevnte åpne topp av nevnte form.

4 2 6. Fremgangsmåte ifølge krav, hvor nevnte kjølemedium er vann eller luft. 7. Fremgangsmåte ifølge krav 1, hvor nevnte hastighet av ensrettet størkning fastsettes for å minimere dendrittdannelse. 8. Fremgangsmåte ifølge krav 7, hvor nevnte hastighet av ensrettet størkning er lavere enn 1x10-4 m/s Fremgangsmåte ifølge krav 7, hvor nevnte hastighet av ensrettet størkning er omfattet mellom 1x10-4 m/s og x10-6 m/s. 10. Fremgangsmåte ifølge krav 1, hvor det å stanse den ensrettede størkningen gjøres når 40 til 80% av smelten har størknet Fremgangsmåte ifølge krav 1, hvor det å danne en åpning i nevnte ytre skall av nevnte støpeblokk i trinn (e) omfatter å gjennomhulle nevnte ytre skall av nevnte støpeblokk med mekaniske midler eller termisk spyd Fremgangsmåte ifølge krav 1, hvor det å danne en åpning i nevnte ytre skall av nevnte støpeblokk i trinn (e) oppnås gjennom en tappeåpning i nevnte form. 13. Fremgangsmåte ifølge krav 1, hvor nevnte fremgangsmåte videre omfatter et ytterligere trinn før trinn (e) med å fjerne nevnte støpeblokk fra nevnte form Fremgangsmåte ifølge krav 1, hvor nevnte fremgangsmåte videre omfatter et ytterligere trinn (f) med å smelte nevnte faste polykrystallinske silisium med høyere renhet og gjenta trinnene (b) til (e) Fremgangsmåte ifølge krav 1, hvor en øvre andel av nevnte faste polykrystallinske silisium med høyere renhet inneholder minst 90% mindre metallkontaminanter Al, As, Ba, Bi, Ca, Cd, Co, Cr, Cu, Fe, K, La, Mg, Mn, Mo, Na, Ni, Pb, Sb, Sc, Sn, Sr, Ti, V, Zn og Zr enn nevnte silisium av metallurgisk kvalitet med lav renhet. 3

5 3 16. Fremgangsmåte ifølge krav 1, hvor nevnte faste polykrystallinske silisium med høyere renhet inneholder omtrent minst 4% mindre fosfor og omtrent minst 10% mindre bor enn nevnte silisium av metallurgisk kvalitet med lav renhet. 17. Fremgangsmåte ifølge krav 1, hvor nevnte urenhet-anrikede flytende silisium inneholder mindre enn 60 ppm karbon og mindre enn 20 ppm oksygen og er en silisiumkvalitet med lite karbon og lite oksygen.

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