(12) Translation of european patent specification

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1 (12) Translation of european patent specification (11) NO/EP B1 (19) NO NORWAY (1) Int Cl. B01J 23/89 ( ) B01J 21/12 ( ) B01J 23/7 ( ) B01J 37/02 ( ) B01J 37/08 ( ) B01J 37/14 ( ) B01J 37/18 ( ) C07C 1/04 ( ) C10G 2/00 ( ) Norwegian Industrial Property Office (21) Translation Published (80) Date of The European Patent Office Publication of the Granted Patent (86) European Application Nr (86) European Filing Date (87) The European Application s Publication Date (30) Priority , ZA, (84) Designated Contracting States: AL AT BE BG CH CY CZ DE DK EE ES FI FR GB GR HR HU IE IS IT LI LT LU LV MC MK MT NL NO PL PT RO RS SE SI SK SM TR (73) Proprietor Sasol Technology (Proprietary) Limited, 1 Sturdee Avenue Rosebank, 2196 Johannesburg, ZA-Sør-Afrika (72) Inventor VAN RENSBURG, Hendrik, 23 Meadowside Road, Cupar, Fife KY1 DD, GB- Storbritannia (74) Agent or Attorney Oslo Patentkontor AS, Postboks 7007 Majorstua, 0306 OSLO, Norge (4) Title PROCESS FOR PREPARING A COBALT - CONTAINING FISCHER TROPSCH CATALYST (6) References Cited: WO-A2-2010/0716 WO-A2-2010/09774 US-A US-B

2 Enclosed is a translation of the patent claims in Norwegian. Please note that as per the Norwegian Patents Acts, section 66i the patent will receive protection in Norway only as far as there is agreement between the translation and the language of the application/patent granted at the EPO. In matters concerning the validity of the patent, language of the application/patent granted at the EPO will be used as the basis for the decision. The patent documents published by the EPO are available through Espacenet (http://worldwide.espacenet.com) or via the search engine on our website here: https://search.patentstyret.no/ NO/EP278170

3 1 Patentkrav 1. Fremgangsmåte for fremstilling av en katalysator for hydrokarbonsyntese inneholdende kobolt, der fremgangsmåten omfatter kalsinering av et utgangsmateriale for katalysatorforløper støttende den koboltforbindelse, med varmebehandling av utgangsmateriale for katalysatorforløper under ikke-reduserende betingelser for å dekomponere koboltforbindelsen og/eller få koboltforbindelsen til å reagere med oksygen, derigjennom å oppnå et kalsinert utgangsmateriale for katalysatorforløper; - introdusere koboltforbindelse på og/eller i kalsinert utgangsmateriale for katalysatorforløper slik at kalsinert utgangsmateriale for katalysatorforløper støtter denne koboltforbindelse derigjennom oppnår en påfølgende katalysatorforløper; og - direkte utsette påfølgende katalysatorforløper for reduserende betingelser uten først å utsette den for varmebehandling under oksiderende betingelser noe som medfører oksidering av den støttede koboltforbindelsen eller dekomponering av koboltforbindelsen, til aktivering av den påfølgende katalysatorforløperen, derigjennom å oppnå en katalysator for hydrokarbonsyntese inneholdende kobolt Fremgangsmåte ifølge krav 2, inkluderende istandgjøring katalysatorforløper ved å introdusere koboltforbindelsen på eller/og i katalysatorstøtten. 3. Fremgangsmåte ifølge ethvert av kravene 1 og 2, hvor kalsineringen av utgangsmateriale for katalysatorforløperutføres under oksiderende betingelser, ved en temperatur over 9 C men ikke over 400 C Fremgangsmåte ifølge ethvert av kravene 1 til 3, hvor koboltforbindelsen, introdusert på eller i kalsinert utgangsmateriale for katalysatorforløper, er samme koboltforbindelse som i utgangsmateriale for katalysatorforløper.. Fremgangsmåte ifølge krav 4, hvor koboltforbindelsen er Co(NO 3 ) 2 6H 2 O Fremgangsmåte ifølge ethvert av kravene 1 og, hvor introdusere koboltforbindelsen på eller/og i den kalsinerte katalysatorstøtten skjer ved slurryfase- impregnering.

4 2 7. Fremgangsmåte ifølge krav 6, hvor slurryfaseimpregneringen foregår ved et subatmosfærisk trykk under 8 kpa(a), og ved en temperatur over 2 C men ikke over 9 C. 8. Fremgangsmåte ifølge ethvert av kravene 6 og 7, hvor slurryfaseimpregneringen følges av delvis tørking av det impregnerte, kalsinerte utgangsmateriale for katalysatorforløper, ved en tørkingstemperatur over 2 C og ved et subatmosfærisk trykk under 8 kpa(a) Fremgangsmåte ifølge ethvert av kravene 1 til 8, hvor utsetting av den påfølgende katalysatorforløperen for reduserende betingelser inkluderer å utsette den påfølgende katalysatorforløperen for en reduserende gass, derigjennom å aktivere den påfølgende katalysatorforløperen Fremgangsmåte ifølge ethvert av kravene 1 til, hvor introduksjonen av koboltforbindelsen på og/eller i det kalsinerte utgangsmateriale for katalysatorforløper er ved impregnering, omfattende danning av en blanding med koboltforbindelsen, et flytende bærer for koboltforbindelsen, og det kalsinerte utgangsmateriale for katalysatorforløper, og tørke den resulterende impregnerte, kalsinerte utgangsmateriale for katalysatorforløper ved en temperatur over 2 C, for å få den påfølgende katalysatorforløper En fremgangsmåte ifølge krav 10, hvor utsetting av den påfølgende katalysatorforløperen for reduserende betingelser inkluderer å utsette den påfølgende katalysatorforløperen for en reduserende gass, derigjennom aktivere den påfølgende katalysatorforløperen, hvor den påfølgende katalysatorforløperen er omtrent ved tørketemperatur når påfølgende katalysatorforløperen utsettes for den reduserende gassen En fremgangsmåte ifølge ethvert av kravene 9 eller 11, hvor den reduseren- de gassen er hydrogen eller en gass inneholdende hydrogen En fremgangsmåte ifølge ethvert av kravene 9, 11 eller 12, hvor den påfølgende katalysatorforløperen utsettes for den reduserende gassen gjennom en fremgangsmåte hvor gassen blåses en beholder med partikler av den påfølgende katalysatorforløperen.

5 3 14. En fremgangsmåte for fremstilling av hydrokarboner, der fremgangsmåten omfatter istandgjøring en koboltinneholdende katalysator for hydrokarbonsyntese ifølge ethvert av kravene 1 til 13; og føre hydrogen i kontakt med karbonmonoksid ved en temperatur over 100 C og et trykk på minst 10 bar ved tilstedeværelse av koboltinneholdende katalysator for hydrokarbonsyntese, derigjennom fremstille hydrokarboner i en Fischer-Tropsch synteseprosess.

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